HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 483869Generated: October 30, 2026
Acetyl chloride → HCID 131718027, compound
https://huagongshe.com/reaction/483869
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Acetyl chloride | HCID 6367 | — |
| Reactant | Aluminum(III) Chloride | HCID 6451240 | — |
| Reactant | 1~4~,3~4~-Dibromo-1~1~,2~1~:2~2~,3~1~-terphenyl | HCID 12715106 | — |
| Solvent | Nitrobenzene | HCID 7416 | — |
| Product | HCID 131718027 | HCID 131718027 | — |
Reaction Steps
To 3.8 (0.01 mole) 4,4"-dibromoterphenyl in 200 ml nitrobenzene is added 0.86 g (0.011 mole) acetyl chloride and 1.46 g (0.011 mole) aluminum trichloride. The mixture is heated to 80° C. under inert atmosphere for three hours. The mixture is cooled to room temperature and washed with 1 m HCl. The organic layer of 2'-acetyl-4,4"-dibromoterphenyl is separated and the solids filtered and washed with several portions of ethanol, and dried.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05227457 |
|---|
| Source dataset | uspto-grants-1993_07 |
|---|
| ORD ID | ord-59e0a2bf2d4d466188aff698737e3fd1 |
|---|
| Source note | uspto-grants-1993_07 |
|---|
