HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53411290, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(3-Chlorophenyl)prop-2-enoic acid | HCID 74631 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | HCID 53411290 | HCID 53411290 | — |
Reaction Steps
100 ml of benzene was added to 18.3 grams of m-chlorocinnamic acid. 12 ml of thionyl chloride was added dropwise slowly thereto at ambient temperature. The temperature was elevated to 80° C. and the heating was continued until foaming ceased. Benzene and thionyl chloride were distilled off and the residue was dried thoroughly under reduced pressure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229002 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-05381250536a4912991c8429137f6a18 |
| Source note | uspto-grants-1993_07 |