HuagongsheHuagongshe Chemistry Print Report · For research reference only
Fumaric Acid → Ethanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Fumaric Acid | HCID 444972 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethanol | HCID 702 | 68.3% |
| Product | Fumarate | HCID 5460307 | — |
Reaction Steps
Fumarate is prepared from 6.3 g (0.0158 mol) of base in 100 ml of ethanol and 1.83 g (0.0158 mol) of fumaric acid in 180 ml of ethanol. The clear solution obtained is concentrated almost completely, ethyl acetate is added and the mixture is triturated. A white solid is obtained, which product is recrystallised in ethanol (68.3% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229392 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-96e4f45e874f4c689dd0359f4a422fed |
| Source note | uspto-grants-1993_07 |