HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → 3-(Bromomethyl)biphenyl
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | 3-Methylbiphenyl | HCID 12564 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Solvent | Carbon Tetrachloride | HCID 5943 | — |
| Product | 3-(Bromomethyl)biphenyl | HCID 3864405 | — |
Reaction Steps
3-Phenylbenzyl bromide (melting point 54°-56° C.) was prepared by illumination of a solution of 3-phenyltoluene and N-bromosuccinimide in carbon tetrachloride in the presence of azobisisobutyronitrile.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229393 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-fcf1d89feba149748bfeca870730ee23 |
| Source note | uspto-grants-1993_07 |