HCID 19749645, compound → HCID 19749619, compound

HRID 484059Notes

Reaction equation

HRID 484059 reaction equation
Cl.[S:2]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[N:4]=[C:3]1[N:11]1[CH2:16][CH2:15][CH:14]([CH2:17][NH2:18])[CH2:13][CH2:12]1>[OH-].[Na+]>[S:2]1[C:6]2[CH:7]=[CH:8][CH:9]=[CH:10][C:5]=2[N:4]=[C:3]1[N:11]1[CH2:12][CH2:13][CH:14]([CH2:17][NH2:18])[CH2:15][CH2:16]1

Participants

3

Reactant 1

HCID 19749645HCID 19749645, compound

Product 1

HCID 19749619HCID 19749619, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

The compound of Example 1 is taken up in 1N caustic soda. The expected product is then obtained after extraction with dichloromethane. After drying, the organic phase is filtered and evaporated. The oil thus obtained is taken up in boiling hexane. After cooling, the product crystallizes.

Sources & evidence

ORD record
ord-6c7dc7bad0a044a1b17c3813c51c49f6
Source dataset
uspto-grants-1993_07
Patent number
US05229398

Reaction notes

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