HCID 19749671, compound → HCID 19749683, compound

HRID 484073Notes

Reaction equation

HRID 484073 reaction equation
[CH:1]1[C:11]2[CH:10]=[CH:9][C:8]3[CH:12]=[CH:13][CH:14]=[CH:15][C:7]=3[C:6](=[C:16]3[CH2:21][CH2:20][N:19]([CH2:22][CH2:23][CH2:24][C:25]4[CH:30]=[CH:29][C:28]([N+:31]([O-])=O)=[CH:27][CH:26]=4)[CH2:18][CH2:17]3)[C:5]=2[CH:4]=[CH:3][CH:2]=1>[Zn]>[NH2:31][C:28]1[CH:27]=[CH:26][C:25]([CH2:24][CH2:23][CH2:22][N:19]2[CH2:20][CH2:21][C:16](=[C:6]3[C:5]4[CH:4]=[CH:3][CH:2]=[CH:1][C:11]=4[CH:10]=[CH:9][C:8]4[CH:12]=[CH:13][CH:14]=[CH:15][C:7]3=4)[CH2:17][CH2:18]2)=[CH:30][CH:29]=1

Participants

3

Reactant 1

HCID 19749671HCID 19749671, compound2×

Product 1

HCID 19749683HCID 19749683, compoundYield 97.3%

Reagents, catalysts & solvents 1

HCID 23994ZincCatalyst

Procedure

3-[4-(5H-Dibenzo[a,d]cyclohepten-5-ylidene)-1-piperidinyl]-1-(4-nitrophenyl)propane (compound 7) was reduced by zinc. Yield 97.3%.

Sources & evidence

ORD record
ord-e5294f8758234735a6fc221a1e8afb23
Source dataset
uspto-grants-1993_07
Patent number
US05229400

Reaction notes

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