Acetic Anhydride → HCID 22990733, compound

HRID 484074Notes

Reaction equation

[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([CH2:8][CH2:9][CH2:10][N:11]2[CH2:16][CH2:15][C:14](=[C:17]3[C:23]4[CH:24]=[CH:25][CH:26]=[CH:27][C:22]=4[CH:21]=[CH:20][C:19]4[CH:28]=[CH:29][CH:30]=[CH:31][C:18]3=4)[CH2:13][CH2:12]2)=[CH:4][CH:3]=1.[C:32](OC(=O)C)(=[O:34])[CH3:33]>>[C:32]([NH:1][C:2]1[CH:3]=[CH:4][C:5]([CH2:8][CH2:9][CH2:10][N:11]2[CH2:16][CH2:15][C:14](=[C:17]3[C:18]4[CH:31]=[CH:30][CH:29]=[CH:28][C:19]=4[CH:20]=[CH:21][C:22]4[CH:27]=[CH:26][CH:25]=[CH:24][C:23]3=4)[CH2:13][CH2:12]2)=[CH:6][CH:7]=1)(=[O:34])[CH3:33]

Participants

Reactant 2

HCID 7918Acetic Anhydride

HCID 19749683HCID 19749683, compound2×

Product 1

HCID 22990733HCID 22990733, compoundYield 92.9%

Procedure

This was prepared from 1-(4-Aminophenyl)-3-[4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)-1-piperidinyl]propane (compound 8) and acetic anhydride. Yield 92.9%

Sources & evidence

ORD record: ord-b890edfb51c046479b625a3c6c90f7de
Source dataset: uspto-grants-1993_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05229400

Reaction notes

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