Ethyl chloroformate → HCID 54382113, compound

HRID 484080Notes

Reaction equation

HRID 484080 reaction equation
[NH2:1][C:2]1[CH:31]=[CH:30][C:5]([CH:6]=[CH:7][CH2:8][N:9]2[CH2:14][CH2:13][C:12](=[C:15]3[C:21]4[CH:22]=[CH:23][CH:24]=[CH:25][C:20]=4[CH:19]=[CH:18][C:17]4[CH:26]=[CH:27][CH:28]=[CH:29][C:16]3=4)[CH2:11][CH2:10]2)=[CH:4][CH:3]=1.Cl[C:33]([O:35][CH2:36][CH3:37])=[O:34]>>[CH:25]1[C:20]2[CH:19]=[CH:18][C:17]3[CH:26]=[CH:27][CH:28]=[CH:29][C:16]=3[C:15](=[C:12]3[CH2:11][CH2:10][N:9]([CH2:8][CH:7]=[CH:6][C:5]4[CH:4]=[CH:3][C:2]([NH:1][C:33]([O:35][CH2:36][CH3:37])=[O:34])=[CH:31][CH:30]=4)[CH2:14][CH2:13]3)[C:21]=2[CH:22]=[CH:23][CH:24]=1

Participants

3

Reactant 2

HCID 10928Ethyl chloroformateHCID 53692038HCID 53692038, compound2×

Product 1

HCID 54382113HCID 54382113, compoundYield 56.7%

Procedure

This compound was prepared from 1-(4-Aminocinnamyl)-4-(5H-dibenzo[a,d]cyclohepten-5-ylidene)piperidine (compound 5) and ethyl chloroformate. Yield 56.7%

Sources & evidence

ORD record
ord-35138c39ebc04609b7868516a8a4416f
Source dataset
uspto-grants-1993_07
Patent number
US05229400

Reaction notes

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