HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methoxyphenyl)piperazine → HCID 21706597, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methoxyphenyl)piperazine | HCID 1346 | — |
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 21706621 | HCID 21706621 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 21706597 | HCID 21706597 | — |
Reaction Steps
To a solution of 2,2-dimethyl-3-(4-chlorobutyl)-4-thiazolidinone (3.26 g) and 1-(2-methoxyphenyl)piperazine (2.8 g) in 100 ml of anhydrous CH3CN were added anhydrous K2CO3 (4.5 g) and NaI (200 mg). The mixture was heated with stirring to 80° under N2.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229388 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-13dc1d85d7654d46bd855d14c86464cd |
| Source note | uspto-grants-1993_07 |