HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → HCID 20090007, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | 1-BENZYL-1,2,3,6-TETRAHYDROPYRIDINE | HCID 6421573 | — |
| Catalyst | zinc(II)iodide | HCID 9883512 | — |
| Product | HCID 20090007 | HCID 20090007 | — |
Reaction Steps
Reaction of 1-benzyl-1,2,5,6-tetrahydropyridine with diazomethane and zinc iodide, according to the method of Attia, Ind. J. Chem., 16B, 98 (1978) provides 3-benzyl-3-azabicyclo[4.1.0]heptane. Hydrogenolytic removal of the benzyl group gives 3-azabicyclo[4.1.0]heptane.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229396 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-d51b95cbd9d64cd9a2a854e698fcae7e |
| Source note | uspto-grants-1993_07 |