HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Benzyloxy-a-methyl carbazole-2-acetic acid ethyl ester → HCID 54544615, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Benzyloxy-a-methyl carbazole-2-acetic acid ethyl ester | HCID 54110684 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 54544615 | HCID 54544615 | 90.5% |
Reaction Steps
A mixture consisting of 6-benzyloxy-α-methyl carbazole-2-acetic acid ethyl ester (7.3 g, 0.0195 mol) and ethanol (130 mL) is subjected to hydrogenation over 10% Pd/c (0.9 g) for 18 hours at 35 psi. The reaction mixture is filtered and concentrated to give 5.0 g product as a foam.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05229516 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-935d608c6ae248f2bfe8a0a643170473 |
| Source note | uspto-grants-1993_07 |