HuagongsheHuagongshe Chemistry Print Report · For research reference only
Tetradecyl 4-hydroxybenzoate → Ethyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Tetradecyl 4-hydroxybenzoate | HCID 328882 | — |
| Reactant | n-Tetradecyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate | HCID 19748003 | — |
| Product | Ethyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate | HCID 19748015 | — |
Reaction Steps
n-Tetradecyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate-Using n-tetradecyl 4-hydroxybenzoate, the title compound was synthesized as a colorless oil. PMR (CDCl3): δ 0.83-0.94 (3H, m), 1.15-1.50 (34H, m), 1.70-1.85 (6H, m), 4.34 (2H, t, J~6.7 Hz), 7.29 (2H, d, J~8.7 Hz), 7.46 (1H, d, J~8.4 Hz), 7.95 (1H, dd, J~8.4 Hz, 1.8 Hz), 8.14 (2H, d, J~8.7 Hz), 8.16 (1H, d, J~1.8 Hz).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05231113 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-c877d8db483b4bc796754bf0b461430d |
| Source note | uspto-grants-1993_07 |