HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxybenzaldehyde → Ethyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxybenzaldehyde | HCID 126 | — |
| Reactant | HCID 19888668 | HCID 19888668 | — |
| Product | Ethyl 4-(5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoyloxy)benzoate | HCID 19748015 | — |
Reaction Steps
4-Formylphenyl 5,5,8,8-tetramethyl-5,6,7,8-tetrahydro-2-naphthoate-Using 4-hydroxybenzaldehyde, the title compound was synthesized as a white solid. PMR (CDCl3): δ 1.32 (6H, d), 1.34 (6H, s), 1.73 (4H, s), 7.39 (2H, d, J~9.0 Hz), 7.45 (1H, d, J~8.4 Hz), 7.92-7.98 (3H, m), 8.16 (1H, d, J~1.8 Hz), 9.99 (1H, s).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05231113 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-30372380d94c400ea460c278a1b67564 |
| Source note | uspto-grants-1993_07 |