HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 10090356, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 10315754 | HCID 10315754 | — |
| Catalyst | Dimethylformamide | HCID 6228 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 10090356 | HCID 10090356 | 101.1% |
Reaction Steps
A mixture of 20 g of m-tetradecyloxyphenylacetic acid, 10.93 g of oxalyl chloride and 41.95 mg of N,N-dimethylformamide in 250 ml of methylene chloride is stirred at ambient temperature for 5 hours. The solvent is removed and the concentrate dissolved in 1:1 ether:hexane and filtered through diatomaceous earth. The filtrate is evaporated to give 21.3 g of the desired product as a light yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05231182 |
| Source dataset | uspto-grants-1993_07 |
| ORD ID | ord-4ce4cee03469498b830761e30a2aa0a8 |
| Source note | uspto-grants-1993_07 |