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HRID484676

反应详情

EQUATION

反应方程式

HRID 484676 的结构方程式

REACTANTS

反应物

1
结构：CCN1CCN(C(=O)NC(C(=O)N[C@@H]2C(=O)N(OCc3ccccc3)[C@H]2C)c2ccccc2)C(=O)C1=O
HCID13036845

未命名化合物

PRODUCTS

生成物

1
结构：CCN1CCN(C(=O)NC(C(=O)N[C@@H]2C(=O)N(O)[C@H]2C)c2ccccc2)C(=O)C1=O
HCID56621498

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

2
结构：[Pd]
催化剂HCID23938

Palladium

Pd

结构：CCO
溶剂HCID702

Ethanol

C2H6O

PROCEDURE

实验过程

(3S-trans)-3-[[[[(4-ethyl-2,3-dioxo-1-piperazinyl)carbonyl]amino]phenylacetyl]amino]-4-methyl-1-(phenylmethoxy)-2-azetidinone (0.270 g) is dissolved in ethanol (25 ml) and hydrogenated over 10% palladium on charcoal catalyst (130 mg) for two hours. The reaction mixture is filtered and concentrated to a solid (0.220 g).

WORKUP

后处理

  1. filtrationThe reaction mixture is filtered
  2. concentrationconcentrated to a solid (0.220 g)