Ethyl chloroformate → HCID 70466361, compound

HRID 484797Notes

Reaction equation

[Cl:1][C:2]([O:4][CH2:5][CH3:6])=[O:3].Cl.Cl.[CH3:9][C:10]1[CH:15]=[C:14]([NH2:16])[CH:13]=[CH:12][C:11]=1[NH:17][C:18]1[CH2:23][CH2:22][CH2:21][CH2:20][N:19]=1>>[ClH:1].[CH3:9][C:10]1[CH:15]=[C:14]([NH:16][C:2]([O:4][CH2:5][CH3:6])=[O:3])[CH:13]=[CH:12][C:11]=1[NH:17][C:18]1[CH2:23][CH2:22][CH2:21][CH2:20][N:19]=1

Participants

Reactant 2

HCID 10928Ethyl chloroformate

HCID 70465507HCID 70465507, compound

Product 1

HCID 70466361HCID 70466361, compound

Procedure

The title compound was prepared by the method of Example 21 using 30.5 mmole of ethyl chloroformate and 1.0 g (3.6 mmole) of the product compound of Example 14. Structure assignment was supported by the nmr spectrum and by elemental analysis.

Sources & evidence

ORD record: ord-f6502b029a3e47dea97c29de50f5eb28
Source dataset: uspto-grants-1985_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04533739

Reaction notes

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