HCID 13199345, compound → HCID 13574634, compound

HRID 484824Notes

Reaction equation

HRID 484824 reaction equation
[CH3:1][C:2]1[C:3]([S:12][CH3:13])=[C:4]([OH:11])[C:5]([S:9][CH3:10])=[C:6]([CH3:8])[CH:7]=1.[CH3:14][S:15]C1C=C(SC)C=CC=1O>>[CH3:1][C:2]1[C:3]([S:12][CH3:13])=[C:4]([OH:11])[C:5]([S:9][CH3:10])=[C:6]([CH3:8])[C:7]=1[S:15][CH3:14]

Participants

3

Reactant 2

HCID 13199345HCID 13199345, compoundHCID 20272427HCID 20272427, compound

Product 1

HCID 13574634HCID 13574634, compound

Procedure

NMR shows fraction 2 to be a mixture of about 90:10 of 3,5-dimethyl-2,6-bis(methylthio)phenol and 2,4-bis(methylthio)phenol.

Sources & evidence

ORD record
ord-2ab90fe14449491782a51d3dc6c969c6
Source dataset
uspto-grants-1985_08
Patent number
US04533753

Reaction notes

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