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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 484895Generated: October 30, 2026

Hydrochloric Acid → HCID 20135909, compound

https://huagongshe.com/reaction/484895

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 20135888HCID 20135888—
SolventEthanolHCID 702—
ProductHCID 20135909HCID 20135909—

Reaction Steps

In 50 ml of absolute ethyl alcohol was dissolved 4.0 g of the 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-7-iodoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-7-iodoindazole dihydrochloride having the following analytical value.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04533731
Source datasetuspto-grants-1985_08
ORD IDord-8b17a9ebab4040a0817223b23cc72d9f
Source noteuspto-grants-1985_08