HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20272264, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 20135876 | HCID 20135876 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20272264 | HCID 20272264 | — |
Reaction Steps
In 20 ml of absolute ethyl alcohol was dissolved 2.5 g of the 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-5,7-diaminoindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-diethylaminopropyl)-3-(3-diethylaminopropylamino)-5,7-diaminoindazole tetrahydrochloride having the following analytical value.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04533731 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-1a3fecb9c512447e97256b92bc96ba6b |
| Source note | uspto-grants-1985_08 |