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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 484900Generated: October 30, 2026

Hydrochloric Acid → HCID 20135764, compound

https://huagongshe.com/reaction/484900

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantDiethyl EtherHCID 3283—
ReactantHCID 13210613HCID 13210613—
SolventEthanolHCID 702—
ProductHCID 20135764HCID 20135764—

Reaction Steps

In 50 ml of absolute ethyl alcohol was dissolved 4.0 g of the 1-(3-piperidinopropyl)-3-(3-diethylaminopropylamino)-5-hydroxyindazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 1-(3-piperidinopropyl)-3-(3-diethylaminopropylamino)-5-hydroxyindazole dihydrochloride having the following analytical value.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04533731
Source datasetuspto-grants-1985_08
ORD IDord-8963208195f04685abb25711e1633fa6
Source noteuspto-grants-1985_08