HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 20135842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | Indazole, 3-((3-morpholinopropyl)amino)- | HCID 3065651 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20135842 | HCID 20135842 | — |
Reaction Steps
In 15 ml of absolute ethyl alcohol was dissolved 1.0 g of the 3-(3-morpholinopropylamino)indazole, and into the solution was introduced dried hydrogen chloride gas under cooling with ice. Then to the solution was added anhydrous diethyl ether to separate crystals. The crystals were obtained by filtration and dried to give 3-(3-morpholinopropylamino)indazole hydrochloride having the following analytical value.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04533731 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-d25f2f454ce7457fb7b1120fe2204575 |
| Source note | uspto-grants-1985_08 |