HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethylparaben → Ethyl 4-hydroxycyclohexanecarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethylparaben | HCID 8434 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Product | Ethyl 4-hydroxycyclohexanecarboxylate | HCID 86973 | — |
Reaction Steps
Into an autoclave is placed ethyl-p-hydroxybenzoate (495 grams) and 5% palladium on carbon (4 grams). The reaction mass is hydrogenated at 150° C. and 50-75 psig hydrogen pressure. After five hours, a sample showed 40% ketone and 44% alcohol having the structure: ##STR24##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04534890 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-992486ea1bf844d282a083150db072df |
| Source note | uspto-grants-1985_08 |