HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Methyl phenyl(4-pyridylmethylthio)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Sodium phenyl(4-picolylthio)acetate | HCID 23686690 | — |
| Product | Methyl phenyl(4-pyridylmethylthio)acetate | HCID 20271275 | — |
Reaction Steps
Sodium phenyl-(4-picolylthio)acetate was dissolved in methanol and dry hydrogen chloride added slowly so as to maintain gentle reflux for 1 hour. After cooling and stirring for approximately 16 hours, the reaction mixture was filtered and concentrated to yield methyl phenyl(4-pyridylmethylthio)acetate (11.6 g.; oil; ms, calcd.: m/e 273; found: 273, 214, 150, 136, 124, 121, 105, 77, 65).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04535084 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-04793db13ec940a4bfd4c463f98da895 |
| Source note | uspto-grants-1985_08 |