HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 485070Generated: October 30, 2026
HCID 178490397, compound → BENZYL ALCOHOL, o-(5-(m-METHOXYPHENYL)-s-TRIAZOL-3-YL)-
https://huagongshe.com/reaction/485070
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | HCID 178490397 | HCID 178490397 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | BENZYL ALCOHOL, o-(5-(m-METHOXYPHENYL)-s-TRIAZOL-3-YL)- | HCID 53228 | — |
Reaction Steps
A suspension of 16 g of 4-[2-(3-methoxybenzyliden)hydrazino]-1H-2,3-benzoxazine in 160 ml of anhydrous xylene is refluxed for 45 minutes and then cooled to about 0° C. The solid which precipitates is recovered by filtration and recrystallized from ethanol yielding 14.7 g of the compound of the title. M.p. 157°-59° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04535090 |
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| Source dataset | uspto-grants-1985_08 |
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| ORD ID | ord-f7ea1029ef8f4c368db77e2b0d8630c9 |
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| Source note | uspto-grants-1985_08 |
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