HCID 13332658, compound → HCID 20271496, compound

HRID 485108Notes

Reaction equation

HRID 485108 reaction equation
[OH:1][CH2:2][C:3]1[CH:4]=[CH:5][C:6]2[CH:12]=[CH:11][C:10]3[CH:13]=[C:14]([O:17][CH3:18])[CH:15]=[CH:16][C:9]=3[S:8][C:7]=2[CH:19]=1.OCC1C=CC2C=CC3C=CC=CC=3SC=2C=1>>[CH3:18][O:17][C:14]1[CH:15]=[CH:16][C:9]2[S:8][C:7]3[CH:19]=[C:3]([CH:2]=[O:1])[CH:4]=[CH:5][C:6]=3[CH:12]=[CH:11][C:10]=2[CH:13]=1

Participants

3

Reactant 2

HCID 13332658HCID 13332658, compoundHCID 20271498HCID 20271498, compound

Product 1

HCID 20271496HCID 20271496, compound

Procedure

Repeat the procedure of Example 4, substituting an equivalent quantity of 3-hydroxymethyl-8-methoxydibenzo[b,f]thiepin for the 3-hydroxymethyldibenzo[b,f]thiepin to obtain the title product.

Sources & evidence

ORD record
ord-d02d24a88aef49fbaa1b660a61017fe7
Source dataset
uspto-grants-1985_08
Patent number
US04535171

Reaction notes

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