Ethanol → HCID 13092101, compound

HRID 485179Notes

Reaction equation

HRID 485179 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][CH:8]=[C:9]([O:10][CH2:11][CH2:12][C:13]#[N:14])[C:4]=2[CH:3]=C1.C([OH:17])C>>[CH:3]([C:4]1[C:5]([OH:1])=[CH:6][CH:7]=[CH:8][C:9]=1[O:10][CH2:11][CH2:12][C:13]#[N:14])=[O:17]

Participants

3

Reactant 2

HCID 702EthanolHCID 20271557HCID 20271557, compound

Product 1

HCID 13092101HCID 13092101, compound

Procedure

3-(4-Benzofuranyloxy)propionitrile (0.935 g, 8 μM) was dissolved in absolute ethanol (225 ml) and ozonised in an analogous manner to that described in example 5(B) to give 3-(2-formyl-3-hydroxyphenoxy)propionitrile which was recrystallised from ethyl acetate/petrol, m.p. 84°-86° C. (Found: C, 62.56; H, 4.79; N, 6.99. C10H9NO3 requires C, 62.38; H, 4.71; N, 7.33%).

Sources & evidence

ORD record
ord-615354b470d842b391260e9d49606637
Source dataset
uspto-grants-1985_08
Patent number
US04535183

Reaction notes

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