HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Iodide → N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide | HCID 12769237 | — |
| Reactant | N,N-diallyl alpha-bromopropionamide | HCID 13036601 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | N-[[4-bromo-3-[1-(diallylcarbamoyl)ethoxy]phenyl]]-3,4,5,6-tetrahydrophthalimide | HCID 13503503 | — |
Reaction Steps
The reaction mixture was washed with water and dried and the solvent was distilled off to obtain 3.8 g. of N,N-diallyl α-bromopropionamide. The product was admixed with 3.5 g. of N-(4-bromo-3-hydroxyphenyl)-3,4,5,6-tetrahydrophthalimide, 2.2 g. of potassium carbonate, 1.8 g. of potassium iodide and 50 ml. of acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536209 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-bf2d6795dd0b49899e460acfaecd3e6b |
| Source note | uspto-grants-1985_08 |