Thionyl Chloride → HCID 54389166, compound

HRID 485234Notes

Reaction equation

[CH3:1][P:2]([CH2:6][O:7][C:8]1[CH:13]=[C:12]([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][C:16]=2[Cl:25])[CH:11]=[CH:10][C:9]=1[N+:26]([O-:28])=[O:27])(=O)[O:3]C.S(Cl)([Cl:31])=O>>[CH3:1][P:2]([Cl:31])([CH2:6][O:7][C:8]1[CH:13]=[C:12]([O:14][C:15]2[CH:20]=[CH:19][C:18]([C:21]([F:24])([F:23])[F:22])=[CH:17][C:16]=2[Cl:25])[CH:11]=[CH:10][C:9]=1[N+:26]([O-:28])=[O:27])=[O:3]

Participants

Reactant 2

HCID 24386Thionyl Chloride

HCID 70477998HCID 70477998, compound

Product 1

HCID 54389166HCID 54389166, compound

Procedure

Following the procedure of Example 4, methyl P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)-phenoxymethylphosphinate is reacted with thionyl chloride to give P-methyl-2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenoxymethylphosphinic chloride.

Sources & evidence

ORD record: ord-2670318f443143e48e127bbe5416df2f
Source dataset: uspto-grants-1985_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04536355

Reaction notes

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