HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 20256663, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | Dimethyl (1-hydroxyethyl)phosphonate | HCID 112018 | — |
| Reactant | Benzene, 2-chloro-1-(3,4-dinitrophenoxy)-4-(trifluoromethyl)- | HCID 156238 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 20256663 | HCID 20256663 | — |
Reaction Steps
A mixture of 4-(2-chloro-4-trifluoromethylphenoxy)-1,2-dinitrobenzene (600 mg), dimethyl α-hydroxyethylphosphonate (382 mg), potassium carbonate (343 mg) and 2-butanone (8 ml) is heated under reflux for 24 hours. The reaction mixture is filtered, and the filtrate is concentrated and purified by prep. TLC to give dimethyl α-[2-nitro-5-(2-chloro-4-trifluoromethylphenoxy)phenoxy]ethylphosphonate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536355 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-d0b2ef7602274f33aec40fb7f4a5ff71 |
| Source note | uspto-grants-1985_08 |