HuagongsheHuagongshe Chemistry Print Report · For research reference only
Water → N-8-(1-naphthyloxy)octylphthalimide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Water | HCID 962 | — |
| Reactant | 1-(1-Naphthyloxy)-8-chlorooctane | HCID 13957273 | — |
| Reactant | Phthalimide potassium salt | HCID 24194345 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | N-8-(1-naphthyloxy)octylphthalimide | HCID 13520543 | — |
Reaction Steps
A solution of 1-(1-naphthyloxy)-8-chlorooctane (9.5 g) and potassium phthalimide (8.4 g) in dimethylformamide (50 ml) was heated at 140° for 3 hours. The solution was poured into water and extracted with dichloromethane; the extract was washed, dried and evaporated and the residue was crystallized from acetone hexane to afford the intermediate N-8-(1-naphthyloxy)octylphthalimide mp 63°-64°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536503 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-caa8418a47ac42018c68e492fc9f9cbc |
| Source note | uspto-grants-1985_08 |