HuagongsheHuagongshe Chemistry Print Report · For research reference only
Naphthalene, 1,2-dihydro-4-(4-methoxyphenyl)- → HCID 13408690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Naphthalene, 1,2-dihydro-4-(4-methoxyphenyl)- | HCID 12048655 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13408690 | HCID 13408690 | 92.5% |
Reaction Steps
1-(4-Methoxyphenyl)-3,4-dihydro-naphthalene (12 g., 0.051 mole) was added to a mixture of 10% Pd on carbon catalyst (1.0 g.) and ethanol (250 ml.) and hydrogenated for 4 hours at room temperature and 50 psi of H2. The reaction mixture was then filtered and evaporated under vacuum to an oil, which was used in the next step without further purification (11.2 g., 92.5% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536518 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-3a0b375dc49348c39a7faf5906f7ff17 |
| Source note | uspto-grants-1985_08 |