HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → L 636499
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 13151874 | HCID 13151874 | — |
| Solvent | Water | HCID 962 | — |
| Product | L 636499 | HCID 130562 | — |
Reaction Steps
13.6 G. 3-cyanodibenzo[b,f]thiepin-5,5-dioxide are refluxed for 2.5 hours in a mixture of 20 cc. 10% aqueous sodium hydroxide solution and 20 cc. ethanol. The mixture is diluted with water and acidified with concentrated HCl. The acid precipitates as a white solid. The yield of acid, m.p. 268° C.-270° C., is 1.38 g. (94.6%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04536507 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-ac313329c6d54e8f96c9620a6b9b8f9e |
| Source note | uspto-grants-1985_08 |