HRID485422
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
13.5 G. 10,11-dihydro-11-hydroxydibenzo-[b,f]thiepin-3-carboxylic acid is suspended in ether and excess diazomethane is added in portions. A clear solution results which is filtered from small particles in suspension and the filtrate evaporated to dryness to a yellow oil weighing 14.2 g.
WORKUP
后处理
- customA clear solution results which
- filtrationis filtered from small particles in suspension
- customthe filtrate evaporated to dryness to a yellow oil