HRID485422

反应详情

EQUATION

反应方程式

HRID 485422 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

13.5 G. 10,11-dihydro-11-hydroxydibenzo-[b,f]thiepin-3-carboxylic acid is suspended in ether and excess diazomethane is added in portions. A clear solution results which is filtered from small particles in suspension and the filtrate evaporated to dryness to a yellow oil weighing 14.2 g.

WORKUP

后处理

  1. customA clear solution results which
  2. filtrationis filtered from small particles in suspension
  3. customthe filtrate evaporated to dryness to a yellow oil