Dimethylamine → HCID 21272611, compound

HRID 4855Notes

Reaction equation

HRID 4855 reaction equation
[Cl:1][CH2:2][CH2:3][CH:4]1[CH2:18][N:17]([CH3:19])[C:16](=[S:20])[C:15]2[C:6](=[C:7]3[C:12](=[CH:13][CH:14]=2)[CH:11]=[N:10][CH:9]=[CH:8]3)[O:5]1.[CH3:21][NH:22][CH3:23]>>[ClH:1].[CH3:21][N:22]([CH3:23])[CH2:2][CH2:3][CH:4]1[CH2:18][N:17]([CH3:19])[C:16](=[S:20])[C:15]2[C:6](=[C:7]3[C:12](=[CH:13][CH:14]=2)[CH:11]=[N:10][CH:9]=[CH:8]3)[O:5]1

Participants

3

Reactant 2

HCID 674DimethylamineHCID 212714312-(2-chloroethyl)-2,3-dihydo-4-methyl-1,4-oxazepino[7,6-f]isoquinoline-5(4H)-thione

Product 1

HCID 21272611HCID 21272611, compound

Procedure

Following the procedure of Example 31, 2-(2-chloroethyl)-2,3-dihydro-4-methyl-1,4-oxazepino[7,6-f]isoquinoline-5(4H)-thione is reacted with dimethylamine to give the title compound.

Sources & evidence

ORD record
ord-5bc77dfd9e3c45db8eebc1805fbfa2fb
Source dataset
uspto-grants-1988_02
Patent number
US04727152

Reaction notes

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