HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 13338728, compound → HCID 13338729, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 13338728 | HCID 13338728 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13338729 | HCID 13338729 | — |
Reaction Steps
A solution of 7-acetoxy-1,3,4,5,6,7-hexahydro-1-benzazonin-2-one (7.4 g) in ethanol (250 ml) is hydrogenated at 3 atmospheres at 70° using 10% palladium on charcoal (1.5 g) as catalyst. The catalyst is filtered off and the solvent removed under reduced pressure. The residue is recrystallized to give 1,3,4,5,6,7-hexahydro-1-benzazonin-2-one.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04537885 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-ea058813055040c4a405167c18fcf9a0 |
| Source note | uspto-grants-1985_08 |