3-Phenoxybenzyl alcohol → HCID 54463321, compound

Participants

Reaction Steps

Using the procudure of Example 1, 1.2 g of the acid of Example 29 and 1 g of 3-phenoxy-benzyl alcohol were reacted to obtain after chromatography over silica gel and elution with a 9-1 hexane-ethyl acetate mixture 1.49 g of 3-phenoxybenzyl (1R,trans) 2,2-dimethyl-3-(3-bromo-1,2-propadienyl)-cyclopropane-carboxylate with a specific rotation of [α]D20 =+15.5°±2° (c=0.5% in chloroform).

Provenance & Evidence