HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrobenzoyl chloride → HCID 178507637, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrobenzoyl chloride | HCID 8502 | — |
| Reactant | Indazolinone | HCID 81829 | — |
| Reactant | HCID 131714318 | HCID 131714318 | — |
| Product | HCID 178507637 | HCID 178507637 | — |
Reaction Steps
Reaction of 1H-indazol-3-ol with p-nitrobenzoyl chloride and subsequent catalytic reduction of the nitrobenzoyl indazol derivative according to the general procedure B above afforded the desired amine as a colorless solid in 49.1% overall yield; m.p. 233°-235° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04537966 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-5807ef67498e45e9b2d9c372952ee8ae |
| Source note | uspto-grants-1985_08 |