HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorophenol → 4-Chloro-1-(4-chlorophenoxy)-2-butanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorophenol | HCID 4684 | — |
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | 1,4-Dichloro-2-butanol | HCID 17021 | — |
| Solvent | Water | HCID 962 | — |
| Product | 4-Chloro-1-(4-chlorophenoxy)-2-butanol | HCID 13120349 | — |
Reaction Steps
4-Chloro-1-(4-chlorophenoxy)-2-butanol was prepared using the procedure of Preparation 7 from 45 g. (0.5 mole) of p-chlorophenol, 72 g. (0.5 mole) of 1,4-dichloro-2-butanol, 40 g. (1.0 mole) of sodium hydroxide and 400 ml. of water to give 85 g. (36.1%) of product which melted at 62°-64° C. after recrystallization from isopropanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04538001 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-3dd77d3a293b4af8b02f7d5489e7bb9c |
| Source note | uspto-grants-1985_08 |