HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 136399289, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178449351 | HCID 178449351 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 136399289 | HCID 136399289 | — |
Reaction Steps
20 g (58.65 millimols) of tetrachlorophthalic acid N-n-butylimide, 26.49 g (240.5 millimols) of thiophenol, 49.04 g (355 millimols) of potassium carbonate and 200 ml of ethyl acetate are stirred at 25° C. for 18 hours and worked up as described in the preceding examples. After recrystallisation from toluene/cyclohexane, 35.99 g (97% of theory) of tetrakis-(phenylthio)-phthalic acid N-n-butylimide are obtained: melting point 159°-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04537977 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-d7073bd1cbfd4e85ac57d7b65db8024e |
| Source note | uspto-grants-1985_08 |