HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Methylbenzenethiol → HCID 178427278, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Methylbenzenethiol | HCID 7811 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 178524541 | HCID 178524541 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 178427278 | HCID 178427278 | — |
Reaction Steps
20 g (60.8 millimols) of tetrachlorophthalic acid N-2-hydroxyethylimide, 15.86 g (127.67 millimols) of p-thiocresol, 34.03 g (246.22 millimols) of potassium carbonate and 200 ml of tetrahydrofuran are stirred at 25° C. for 2.5 days. The mixture is acidified and extracted with methylene chloride. After recrystallisation from toluene, 26.42 g (86% of theory) of the title compound are obtained; melting point 211°-2° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04537977 |
| Source dataset | uspto-grants-1985_08 |
| ORD ID | ord-97b6450d46d443ce9abd7827d2da3720 |
| Source note | uspto-grants-1985_08 |