反应详情

To a solution of 10 cm3 of acetyl bromide in 150 cm3 of ether, cooled to -20° C., one adds a solution of 26 cm3 of methylisopropylamine in 100 cm3 of ether. One leaves the mixture to return to 20° C. and agitates it for 30 minutes at 20° C. One dilutes with water, decants, extracts with ether, dries and separates by distillation. One obtains 13 g of expected product. B.p.=72°/72° under 1 mmHg.

1. customOne leaves the mixture
2. customto return to 20° C.
3. customfor 30 minutes
4. customat 20° C
5. customdecants
6. distillationextracts with ether, dries and separates by distillation