HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-((2-Chloroethyl)thio)hexane → HCID 178445572, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-((2-Chloroethyl)thio)hexane | HCID 12260279 | — |
| Reactant | 3-Amino-5-{2-[2-(hexylthio)ethylthio]ethylthio}-1,2,4-triazole | HCID 178445574 | — |
| Product | HCID 178445572 | HCID 178445572 | 86% |
Reaction Steps
Compound 6 was prepared using the procedure used for Compound 12, but with 2-chloroethyl hexyl sulfide as the starting material. The yield was 86%. A portion was recrystallized from ligroin/ethyl acetate to obtain a solid, m.p. 76.5°-78° C. Analysis: Calculated for C10H20N4S2 : C, 46.12; H, 7.74; N, 21.51. Found: C, 46.00; H, 7.56; N, 21.56.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292627 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-046e7a63452d490ab3f392038e3f1525 |
| Source note | uspto-grants-1994_03 |