HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Chloroethyl octyl sulfide → HCID 178443886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Chloroethyl octyl sulfide | HCID 12743198 | — |
| Reactant | 3-Amino-5-{2-[2-(hexylthio)ethylthio]ethylthio}-1,2,4-triazole | HCID 178445574 | — |
| Product | HCID 178443886 | HCID 178443886 | 96% |
Reaction Steps
Compound 7 was prepared by using the procedure used for Compound 12, but with 2-chloroethyl octyl sulfide as the starting material. The yield was 96%. A portion was recrystallized from ligroin/ethyl acetate to obtain a solid, m.p. 85°-86° C. Analysis: Calculated for C12H24N4S2 : C, 49.96; H, 8.39; N, 19.42. Found: C, 49.54; H, 8.12; N, 19.29.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292631 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-c7aadedebb3346cf9f510ffd59f2afdc |
| Source note | uspto-grants-1994_03 |