HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 67851899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Sodium Sulfite | HCID 24437 | — |
| Reactant | 4-Chloro-3-(chlorosulphonyl)benzoic acid | HCID 75613 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 67851899 | HCID 67851899 | — |
Reaction Steps
is obtained from 186 g of 5-carboxy-2-chlorobenzenesulfinic acid, prepared by reduction of 261 g of 5-carboxy-2-chlorobenzenesulfonyl chloride with 157 g of sodium sulfite in 700 ml of water at 70° C. at pH 9-10 and subsequent acidification using HCl, by neutralization with 67.6 g of caustic soda in 2 liters of water, removal of the latter by distillation and crystallization of the residue with acetone.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292755 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-63a390847d6c495cbf2b69ef11fb6405 |
| Source note | uspto-grants-1994_03 |