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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 486614Generated: October 31, 2026

Lawesson's reagent → HCID 15294850, compound

https://huagongshe.com/reaction/486614

Reaction equation

Participants

RoleNameHCIDCharge
ReactantLawesson's reagentHCID 87949—
ReactantHCID 15294836HCID 15294836—
SolventTolueneHCID 1140—
ProductHCID 15294850HCID 15294850147.6%

Reaction Conditions

Temperature100 °C

Reaction Steps

A mixture of 549 mg (1.371 mmol) of the compound produced in Example 82, 333 mg (0.823 mmol) of Lawesson reagent and 10 ml of toluene was heated at 100° C. After the concentration, the residue was purified by silica gel column chromatography to obtain 506 mg of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05292758
Source datasetuspto-grants-1994_03
ORD IDord-eb08a7317c424e678c7c8357334afb61
Source noteuspto-grants-1994_03