HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 486614Generated: October 31, 2026
Lawesson's reagent → HCID 15294850, compound
https://huagongshe.com/reaction/486614
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Lawesson's reagent | HCID 87949 | — |
| Reactant | HCID 15294836 | HCID 15294836 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 15294850 | HCID 15294850 | 147.6% |
Reaction Steps
A mixture of 549 mg (1.371 mmol) of the compound produced in Example 82, 333 mg (0.823 mmol) of Lawesson reagent and 10 ml of toluene was heated at 100° C. After the concentration, the residue was purified by silica gel column chromatography to obtain 506 mg of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05292758 |
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| Source dataset | uspto-grants-1994_03 |
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| ORD ID | ord-eb08a7317c424e678c7c8357334afb61 |
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| Source note | uspto-grants-1994_03 |
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