HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetylacetone → Orazipone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetylacetone | HCID 31261 | — |
| Reactant | 4-(Methylsulfonyl)benzaldehyde | HCID 220376 | — |
| Product | Orazipone | HCID 178387 | — |
Reaction Steps
The procedure described in Example 1 was repeated by using 1.1 g of 4-methylsulfonylbenzaldehyde and 1.5 g of 2,4-pentanedione. The product was crystallized from ether, mp 139°-140° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292771 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-2dcb663b4baf43b790706ecc020aae57 |
| Source note | uspto-grants-1994_03 |