HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 67819886, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 1-Iodopropane | HCID 33643 | — |
| Reactant | HCID 57294480 | HCID 57294480 | — |
| Product | HCID 67819886 | HCID 67819886 | — |
Reaction Steps
Using the procedure of Example 7D, the reaction of (2aS,4S)-4-amino-1-benzoyl-6-bromo-1,2,2a,3,4,5-hexahydrobenz[cd]indole (5.4 g, 0.015 mol) with n-propyliodide (10.2 g, 0.06 mol) in the present of K2CO3 (8.28 g, 0.06 mol) in 200 ml of CH3CN gave, after chromatography, 3.1 g of product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292766 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-22e4a333fea84846add8975f0a9157b0 |
| Source note | uspto-grants-1994_03 |