HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium hydride → HCID 19926603, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | 5-Bromothiophene-2-carbaldehyde | HCID 78428 | — |
| Reactant | HCID 178418642 | HCID 178418642 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 19926603 | HCID 19926603 | — |
Reaction Steps
25.0 g of 4-hydroxypyridine was suspended in 440 ml of N,N-dimethylformamide. 11.04 g of sodium hydride (60% suspension in mineral oil) was added to the suspension in portions and the suspension was stirred for 1 h. 32.8 ml of 5-bromothiophene-2-carboxaldehyde was added thereto and a reaction was conducted at 120° C. for 4 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292770 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-bc15143cc57c4809b115230b33b1b5ba |
| Source note | uspto-grants-1994_03 |