HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Thioglycolate → HCID 54184237, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Thioglycolate | HCID 12185 | — |
| Reactant | 1,3-Benzodioxole, 5-ethenyl- | HCID 138986 | — |
| Product | HCID 54184237 | HCID 54184237 | 69.1% |
Reaction Steps
3.24 g of ethyl thioglycolate was added to 6 g of 5-ethenyl-1,3-benzodioxole and the mixture was stirred at room temperature for 14 h. The reaction product was purified according to silica gel column chromatography (benzene:ethyl acetate=40:1) to obtain 5 g of the intended compound in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292901 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-d6dc9ef349814038b226df1e5c0b2a18 |
| Source note | uspto-grants-1994_03 |