HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19096832, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Bromo-2-methylaniline | HCID 11423 | — |
| Reactant | HCID 12440797 | HCID 12440797 | — |
| Product | HCID 19096832 | HCID 19096832 | 66.7% |
Reaction Steps
Ethyl 2-(chlorocarbonyl)butanoate (5.8 grams, 0.03 mole), 4-bromo-2-methylaniline (5.0 grams, 0.03 mole) and triethylamine (3.27 grams, 0.03 mole) were reacted under conditions similar to that described for Example I to give 7.4 grams (0.02 mole) of ethyl 2-(4-bromo-2-methylphenylaminocarbonyl)butanoate as a white solid having a melting point of 98° C.-100° C. Elemental analysis of the product indicated the following:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05292937 |
| Source dataset | uspto-grants-1994_03 |
| ORD ID | ord-bdbf5c67862b4253be4df9d70ef3ca54 |
| Source note | uspto-grants-1994_03 |